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Electrochemical Cyanation of Benzothiazole Derivatives (Supporting Information)

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posted on 2025-01-31, 04:49 authored by Towa MORIKOSHI, Mizuki MATSUSE, Shin YONEYAMA, Pengyu XU, Kouichi MATSUMOTO
Benzo[d]thiazole-2-carbonitrile and the related derivatives are important compounds with applications in a variety of chemical fields. In this paper, electrochemically oxidative cyanation of benzothiazole and their derivatives was successfully achieved by using trimethylsilyl cyanide as a cyanide source in n-Bu4NBF4/DMF in the divided cell, in which the corresponding products were obtained in moderate yields. The extensive reaction optimization as well as scope and limitations were investigated in this paper.

Funding

Japan Society for the Promotion of Science

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Corresponding author email address

kmatsumo@chem.kindai.ac.jp

Copyright

© 2025 The Author(s).

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